4-Cyclohexylphenol → HCID 12531894, compound

HRID 1863336Notes

Reaction equation

HRID 1863336 reaction equation
Br[CH:2]([C:7]1[CH:12]=[CH:11][C:10]([O:13][C:14]2[CH:19]=[CH:18][C:17]([C:20]([CH3:23])([CH3:22])[CH3:21])=[CH:16][CH:15]=2)=[CH:9][CH:8]=1)[C:3]([O:5][CH3:6])=[O:4].[CH:24]1([C:30]2[CH:35]=[CH:34][C:33]([OH:36])=[CH:32][CH:31]=2)[CH2:29][CH2:28][CH2:27][CH2:26][CH2:25]1>>[CH:24]1([C:30]2[CH:31]=[CH:32][C:33]([O:36][CH:2]([C:7]3[CH:12]=[CH:11][C:10]([O:13][C:14]4[CH:19]=[CH:18][C:17]([C:20]([CH3:23])([CH3:22])[CH3:21])=[CH:16][CH:15]=4)=[CH:9][CH:8]=3)[C:3]([O:5][CH3:6])=[O:4])=[CH:34][CH:35]=2)[CH2:25][CH2:26][CH2:27][CH2:28][CH2:29]1

Participants

3

Reactant 2

HCID 143274-CyclohexylphenolHCID 20392606HCID 20392606, compound

Product 1

HCID 12531894HCID 12531894, compoundYield 78.8%

Procedure

In a manner similar to Example 16, 7.54 g of methyl α-bromo-α-[p-(p-tert-butylphenoxy)phenyl]acetate was treated with 4.4 g of p-cyclohexylphenol to give 7.44 g of product as a pale yellow glass.

Sources & evidence

ORD record
ord-7449bcfd613b483eb140ea0174cabbd0
Source dataset
uspto-grants-1979_09
Patent number
US04168385

Reaction notes

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