Ammonia → HCID 178441765, compound

HRID 1863366Notes

Reaction equation

HRID 1863366 reaction equation
Cl.CO[C:4](=[NH:9])[C:5]([CH3:8])([CH3:7])[CH3:6].[OH:10][CH2:11][C:12]([CH2:14]O)=O.[NH3:16]>>[C:5]([C:4]1[NH:9][CH:14]=[C:12]([CH2:11][OH:10])[N:16]=1)([CH3:6])([CH3:7])[CH3:8]

Participants

4

Reactant 3

HCID 222AmmoniaHCID 670DihydroxyacetoneHCID 23151530Methyl 2,2-dimethylpropanecarboximidate hydrochloride

Product 1

HCID 178441765HCID 178441765, compound

Procedure

A mixture of 326 gm. of pivalimidic acid methyl ester hydrochloride and 193.5 gm. of 1,3-dihydroxyacetone in 2 liters of liquid ammonia are reacted as desribed in Example 3, giving the desired product, m.p. 212°-221° C.

Workup

  1. additionA mixture of 326 gm

Sources & evidence

ORD record
ord-577a3a4593d04ee285c0b310789f7413
Source dataset
uspto-grants-1979_09
Patent number
US04168964

Reaction notes

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