Hydrazinecarboxylic acid, ethyl ester → HCID 178473580, compound

HRID 1863387Notes

Reaction equation

HRID 1863387 reaction equation
[C:1]([C:5]1[NH:6][CH:7]=[C:8]([CH:10]=O)[N:9]=1)([CH3:4])([CH3:3])[CH3:2].[C:12]([O:16][CH2:17][CH3:18])(=[O:15])[NH:13][NH2:14]>C(O)C>[CH2:17]([O:16][C:12](=[O:15])[NH:13][N:14]=[CH:10][C:8]1[N:9]=[C:5]([C:1]([CH3:2])([CH3:3])[CH3:4])[NH:6][CH:7]=1)[CH3:18]

Participants

4

Reactant 2

HCID 20064Hydrazinecarboxylic acid, ethyl esterHCID 178441764HCID 178441764, compound

Product 1

HCID 178473580HCID 178473580, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A 7.6 gm. portion of 2-tert-butyl-4-imidazolecarboxaldehyde and 5.2 gm. of ethyl carbazate in 100 ml. of ethanol are reacted as described in Example 32 giving the desired product, m.p. 194°-197° C.

Sources & evidence

ORD record
ord-3a0d709606ca41c8b199b85001104a29
Source dataset
uspto-grants-1979_09
Patent number
US04168964

Reaction notes

Loading…