Hydrazinecarboxylic acid, ethyl ester → 3-[2-(Methoxymethyl)-4-imidazolyl]methylene carbazic acid ethyl ester

HRID 1863390Notes

Reaction equation

HRID 1863390 reaction equation
[CH3:1][O:2][CH2:3][C:4]1[NH:5][CH:6]=[C:7]([CH:9]=O)[N:8]=1.[C:11]([O:15][CH2:16][CH3:17])(=[O:14])[NH:12][NH2:13]>>[CH2:16]([O:15][C:11](=[O:14])[NH:12][N:13]=[CH:9][C:7]1[N:8]=[C:4]([CH2:3][O:2][CH3:1])[NH:5][CH:6]=1)[CH3:17]

Participants

3

Reactant 2

HCID 20064Hydrazinecarboxylic acid, ethyl esterHCID 178494683HCID 178494683, compound

Product 1

HCID 1784735823-[2-(Methoxymethyl)-4-imidazolyl]methylene carbazic acid ethyl ester

Procedure

A 19.60 gm. portion of 2-(methoxymethyl)-4-imidazolecarboxaldehyde and 16.02 gm. of ethyl carbazate are reacted as described in Example 32 giving the desired product, m.p. 186°-190° C.

Sources & evidence

ORD record
ord-2b697d839bb04a6cbbd72dc372a49015
Source dataset
uspto-grants-1979_09
Patent number
US04168964

Reaction notes

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