Methyl carbazate → HCID 178502531, compound

HRID 1863425Notes

Reaction equation

HRID 1863425 reaction equation
CC1NC(C2C=CC=CC=2)=N[C:3]=1[C:13]([C:15]1[N:16]=[C:17]([C:21]2[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=2)[NH:18][C:19]=1C)=O.[C:27]([O:31][CH3:32])(=[O:30])[NH:28][NH2:29]>>[CH3:32][O:31][C:27](=[O:30])[NH:28][N:29]=[C:13]([C:15]1[N:16]=[C:17]([C:21]2[CH:22]=[CH:23][CH:24]=[CH:25][CH:26]=2)[NH:18][CH:19]=1)[CH3:3]

Participants

3

Reactant 2

HCID 80519Methyl carbazateHCID 54068466HCID 54068466, compound

Product 1

HCID 178502531HCID 178502531, compoundYield 91%

Procedure

By the method of Example 104, the title product is prepared from methyl-2-phenyl-4-imidazolyl ketone and methyl carbazate. The product is obtained in 91% yield, m.p. 226.5°-227° C.

Workup

  1. customThe product is obtained in 91% yield, m.p. 226.5°-227° C.

Sources & evidence

ORD record
ord-39edd8db8f814aeb9de256faccfe6876
Source dataset
uspto-grants-1979_09
Patent number
US04168964

Reaction notes

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