HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 2-methylacetoacetate → HCID 54046590, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 2-methylacetoacetate | HCID 701 | — |
| Reactant | HCID 11175640 | HCID 11175640 | — |
| Product | HCID 54046590 | HCID 54046590 | — |
Reaction Steps
Ethyl 2-methylacetoacetate and geranyl geranylbromide were reacted each other and treated according to the preceding Example 1, except that the crude product was purified by distillation under reduced pressure in place of the column chromatography method, to obtain a fraction having the boiling point of 177°-180° C./0.9 mmHg as the objective product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04169157 |
| Source dataset | uspto-grants-1979_09 |
| ORD ID | ord-b818fc228c504162b309e903ecf60462 |
| Source note | uspto-grants-1979_09 |