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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1863879Generated: November 1, 2026

Bromotrimethylsilane → HCID 66832668, compound

https://huagongshe.com/reaction/1863879

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBromotrimethylsilaneHCID 76113—
ReactantHCID 86618280HCID 86618280—
ProductHCID 66832668HCID 66832668—

Reaction Conditions

Temperature5 °C

Reaction Steps

Bromotrimethylsilane (43 mL, 0.326 mol) was added dropwise to cyclopropylmethyl-phosphonic acid diisopropyl ester (18.00 g, 81.8 mmol) stirred in a reaction flask chilled to 5° C. The resulting solution was allowed to warm to ambient temperature, stirred for three hours, and then concentrated by rotary evaporation yielding crude cyclopropylmethyl-phosphonic acid bis(trimethylsilyl) ester which was used without further purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07625880B2
Source datasetuspto-grants-2009_12
ORD IDord-d6ab8da0d96644f58c5c221ad668b4f2
Source noteuspto-grants-2009_12