HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Dimethoxyphenylboronic acid → HCID 131727798, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Dimethoxyphenylboronic acid | HCID 2734702 | — |
| Reactant | HCID 131727799 | HCID 131727799 | — |
| Product | HCID 131727798 | HCID 131727798 | — |
Reaction Steps
rac-cis-1-Acetyl-2,3-bis-(4-chloro-phenyl)-6-(3,4-dimethoxy-phenyl)-2,3-dihydro-1H-imidazo[1,2-a]pyridin-5-one was prepared according to general method D by reaction of rac-cis-1-acetyl-2,3-bis-(4-chloro-phenyl)-2,3-dihydro-6-iodo-1H-imidazo[1 2-a]pyridin-5-one with 3,4-dimethoxyphenylboronic acid The compound was isolated by preparative HPLC. The expected product was characterized by LC/MS (M+H) where the mass was observed as 535.16; the expected mass is 534.1. LC/MS indicated a purity of 100% as measured by UV 214 nM.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07625895B2 |
| Source dataset | uspto-grants-2009_12 |
| ORD ID | ord-fdbf77d8cac94446b822cf5abd1fdb79 |
| Source note | uspto-grants-2009_12 |