HuagongsheHuagongshe Chemistry Print Report · For research reference only
Glycolic Acid → HCID 69057304, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Glycolic Acid | HCID 757 | — |
| Reactant | HCID 69058749 | HCID 69058749 | — |
| Product | HCID 69057304 | HCID 69057304 | 73% |
Reaction Steps
The procedure described in Example 3 (preparation of starting materials) was repeated using glycolic acid and 4-[(5-{[(2S)-2-aminopropyl]oxy}quinazolin-4-yl)amino]-2-chlorophenol to give N-[(1S)-2-({4-[(3-chloro-4-hydroxyphenyl)amino]quinazolin-5-yl}oxy)-1-methylethyl]-2-hydroxyacetamide in 73% yield; Mass spectrum MH+ 403.0.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07625908B2 |
| Source dataset | uspto-grants-2009_12 |
| ORD ID | ord-05032caabd3849c6b258e8cd6a42cf1e |
| Source note | uspto-grants-2009_12 |