Triethylamine → HCID 69019947, compound

Participants

Reaction Steps

At room temperature, to a stirred mixture of 5-(4-bromophenyl)-1H-tetrazole (2.15 g, 9.55 mmol) in CH3CN, add 4-methoxybenzyl chloride (1.42 mL, 10.50 mmol) followed by Et3N (1.46 mL, 10.50 mmol) and stir over night. Concentrate the mixture to half the volume and add water (100 mL). Filter the white precipitate and wash with water (100 mL). Dry the material to give 5-(4-bromophenyl)-1-(4-methoxybenzyl)-1H-tetrazole as white flocculent crystals (1.37 g).

Provenance & Evidence