HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1865226Erstellt: 27. Oktober 2026
1-Carbethoxy-4-ethylamino-3-methylpiperidine → 4-Ethylamino-3-methylpiperidine
https://huagongshe.com/reaction/1865226
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | 1-Carbethoxy-4-ethylamino-3-methylpiperidine | HCID 22278900 | — |
| Lösungsmittel | Sodium Hydroxide | HCID 14798 | — |
| Produkt | 4-Ethylamino-3-methylpiperidine | HCID 22278859 | — |
Reaktionsschritte
1-Carbethoxy-4-ethylamino-3-methylpiperidine (2.3 g, 10.74 mmol) was suspended in 5 M NaOH solution (15 ml), stirred at 110° C. for 120 hr, cooled, extracted with ethyl acetate, dried (Na2SO4) and concentrated to dryness to afford 4-ethylamino-3-methylpiperidine. Yield 0.7 g (46%), C8H18N2, m/z 143, (M+1).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US07626032B2 |
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| Quelldatensatz | uspto-grants-2009_12 |
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| ORD ID | ord-e74ab7d9f8e348a1849e47811f1c4ad5 |
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| Quellennotiz | uspto-grants-2009_12 |
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