HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroacetyl chloride → HCID 178463656, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroacetyl chloride | HCID 6577 | — |
| Reactant | O-Toluidine | HCID 7242 | — |
| Reactant | Ethyl isothiocyanate | HCID 10966 | — |
| Product | HCID 178463656 | HCID 178463656 | — |
Reaction Steps
2-[(Z)-Ethylimino]-3-(2-methylphenyl)-thiazolidin-4-one is prepared following Method B and starting from o-tolylamine, chloroacetyl chloride and ethylisothiocyanate. LC-MS: tR=0.59 min, [M+1]+=235, 1H NMR (CDCl3): δ 7.36-7.28 (m, 3H), 7.15-7.10 (m, 1H), 4.01 (s, 2H), 3.41-3.30 (m, 2H), 2.19 (s, 3H), 1.20-1.13 (m, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07626037B2 |
| Source dataset | uspto-grants-2009_12 |
| ORD ID | ord-7c2ae86416bc46e8bbf4c867dcafa6e0 |
| Source note | uspto-grants-2009_12 |