Benzenamine, 3,5-bis(trifluoromethyl)- → HCID 23070355, compound

HRID 1865358Notes

Reaction equation

HRID 1865358 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([OH:11])[C:5](=[CH:9][CH:10]=1)[C:6]([OH:8])=O.[F:12][C:13]([F:26])([F:25])[C:14]1[CH:15]=[C:16]([CH:18]=[C:19]([C:21]([F:24])([F:23])[F:22])[CH:20]=1)[NH2:17]>>[Cl:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([NH:17][C:16]2[CH:18]=[C:19]([C:21]([F:22])([F:23])[F:24])[CH:20]=[C:14]([C:13]([F:12])([F:25])[F:26])[CH:15]=2)=[O:8])=[C:4]([OH:11])[CH:3]=1

Participants

3

Reactant 2

HCID 9480Benzenamine, 3,5-bis(trifluoromethyl)-HCID 787824-Chlorosalicylic acid

Product 1

HCID 23070355HCID 23070355, compoundYield 55.8%

Procedure

Using 4-chlorosalicylic acid and 3,5-bis(trifluoromethyl)aniline as the raw materials, the same operation as the Example 1(1) gave the title compound.

Sources & evidence

ORD record
ord-6e0800f263744097bc4e685cf3544a41
Source dataset
uspto-grants-2009_12
Patent number
US07626042B2

Reaction notes

Loading…