HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloro-3-nitrobenzoic acid → HCID 178524192, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloro-3-nitrobenzoic acid | HCID 7320 | — |
| Reactant | Potassium ethylxanthate | HCID 2735045 | — |
| Product | HCID 178524192 | HCID 178524192 | 66% |
Reaction Steps
2-Mercapto-benzothiazol-5-carboxylic acid (240) (3.5 g, 66%) was synthesized from 4-chloro-3-nitro-benzoic acid, obtained from Fluka, and potassium dithiocarbonate O-ethyl ester, obtained from Lancaster, according to the procedure of Chaudhuri, N. Synth. Commun. 1996, 26, 20, 3783.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07626033B2 |
| Source dataset | uspto-grants-2009_12 |
| ORD ID | ord-6583efe96f2d4598a4b89477c0e91d41 |
| Source note | uspto-grants-2009_12 |