HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl xanthate → HCID 178509540, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl xanthate | HCID 8823 | — |
| Reactant | 3-Amino-4-chlorobenzonitrile | HCID 104464 | — |
| Reactant | Potassium | HCID 5462222 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178509540 | HCID 178509540 | 49% |
Reaction Steps
The title compound was prepared using the method of example 239, starting with 3-amino-4-chloro-benzonitrile (242) (9.0 g, 59.0 mmol), O-ethylxanthic acid, potassium salt (Lancaster, 21.23 g, 132.7 mmol) in DMF (90 mL). 5.6 g (49%) of compound 243 was obtained as a pale brown solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07626033B2 |
| Source dataset | uspto-grants-2009_12 |
| ORD ID | ord-e4148504d6e74ecf9a9257f10c26ee2a |
| Source note | uspto-grants-2009_12 |