3,4,5-Trichloronitrobenzene → HCID 22148766, compound

HRID 1865525Notes

Reaction equation

HRID 1865525 reaction equation
[SH:1][C:2]1[S:3][C:4]2[CH:10]=[CH:9][C:8]([C:11]([OH:13])=[O:12])=[CH:7][C:5]=2[N:6]=1.[Cl:14][C:15]1[CH:20]=[C:19]([N+:21]([O-:23])=[O:22])[CH:18]=[C:17]([Cl:24])[C:16]=1Cl>>[Cl:14][C:15]1[CH:20]=[C:19]([N+:21]([O-:23])=[O:22])[CH:18]=[C:17]([Cl:24])[C:16]=1[S:1][C:2]1[S:3][C:4]2[CH:10]=[CH:9][C:8]([C:11]([OH:13])=[O:12])=[CH:7][C:5]=2[N:6]=1

Participants

3

Reactant 2

HCID 883653,4,5-TrichloronitrobenzeneHCID 178524192HCID 178524192, compound

Product 1

HCID 22148766HCID 22148766, compound

Procedure

2-(2,6-Dichloro-4-nitro-phenylsulfanyl)-benzothiazole-5-carboxylic acid (255) was prepared (100%) from 2-mercapto-benzothiazol-5-carboxylic acid (240) and 1,2,3-trichloro-5-nitrobenzene, obtained from Aldrich, in a similar manner as described in example 251.

Sources & evidence

ORD record
ord-40916a1fee354322aab371d6c5408ebe
Source dataset
uspto-grants-2009_12
Patent number
US07626033B2

Reaction notes

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