反应详情

A mixture of 35.5 g of methyl behenate (18), 19.7 g of 2-morpholinoethanol (17), 270 mg of sodium methoxide and 150 g of toluene was heated under reflux for 6 hours while distilling off the methanol resulting from the reaction. The reaction solution was cooled. By standard aqueous work-up and distilling off toluene, 41.3 g of (2-morpholinoethyl) behenate (Quencher 2) was obtained (yield 91%).

1. temperaturewas heated
2. temperatureunder reflux for 6 hours
3. distillationwhile distilling off the methanol resulting
4. customfrom the reaction
5. temperatureThe reaction solution was cooled
6. distillationBy standard aqueous work-up and distilling off toluene