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HRID1866793

反应详情

EQUATION

反应方程式

HRID 1866793 的结构方程式

REACTANTS

反应物

1
结构：C/C=C/C1=C(C(=O)O)N2C(=O)[C@@H](NC(=O)[C@H](N)c3ccc(O)cc3)[C@H]2SC1.CN(C)C=O
HCID71467943

未命名化合物

PRODUCTS

生成物

1
结构：C/C=C/C1=C(C(=O)O)N2C(=O)[C@@H](NC(=O)[C@H](N)c3ccc(O)cc3)[C@H]2SC1.O
HCID6436628

未命名化合物

收率 78.3%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

The mixture of Cefprozil dimethylformamide solvate (58 gm, obtained in step-II) and water (100 ml) is stirred for 1 hour, filtered, washed with acetone (100 ml) and dried under vacuum at 40-45° C. to give 40 gm of cefprozil monohydrate (containing 10% E-isomer).

WORKUP

后处理

  1. filtrationfiltered
  2. washwashed with acetone (100 ml)
  3. customdried under vacuum at 40-45° C.