HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Chloride → HCID 86594595, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Chloride | HCID 5234 | — |
| Reactant | Ethylamine | HCID 6341 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Ethyl chloroformate | HCID 10928 | — |
| Reactant | HCID 86594596 | HCID 86594596 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86594595 | HCID 86594595 | 22% |
Reaction Steps
4-(2,2,3-Trimethyl-3-penten-1-yl)-2E-butenoic acid 1 eq, ethyl chloroformate 1.5 eq, triethylamine 1.5 eq, ethylamine 1.5 eq as a 2.0M solution in THF, quench with 10% sodium chloride solution, yield=22%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07632531B2 |
| Source dataset | uspto-grants-2009_12 |
| ORD ID | ord-18c09e0db757478cb1338057932e7cbc |
| Source note | uspto-grants-2009_12 |