HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Chloride → HCID 68954890, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Chloride | HCID 5234 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Ethyl chloroformate | HCID 10928 | — |
| Reactant | Cyclopropylamine | HCID 69828 | — |
| Reactant | HCID 86594596 | HCID 86594596 | — |
| Product | HCID 68954890 | HCID 68954890 | 40% |
Reaction Steps
4-(2,2,3-Trimethyl-3-penten-1-yl)-2E-butenoic acid 1 eq, ethyl chloroformate 1.5 eq, triethylamine 1.5 eq, cyclopropylamine 1.5 eq, quench with 10% sodium chloride solution, yield=40%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07632531B2 |
| Source dataset | uspto-grants-2009_12 |
| ORD ID | ord-9eba0fb983ee444fbb21810c874ab0e6 |
| Source note | uspto-grants-2009_12 |