HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 17973396, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Diisopropylamine | HCID 7912 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Ethyl chloroformate | HCID 10928 | — |
| Reactant | trans-3-Methyl-2-hexenoic acid | HCID 6443739 | — |
| Product | HCID 17973396 | HCID 17973396 | 34% |
Reaction Steps
3-Methyl-2E-hexenoic acid 1 eq, ethyl chloroformate 1.5 eq, triethylamine 1.6 eq, diisopropylamine 3.0 eq, quench with 10% hydrogen chloride solution, yield=34%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07632531B2 |
| Source dataset | uspto-grants-2009_12 |
| ORD ID | ord-5da7be764ee34e9dad3d5d429ef81603 |
| Source note | uspto-grants-2009_12 |