HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69055417, compound → HCID 69053624, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69055417 | HCID 69055417 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 69053624 | HCID 69053624 | 85.1% |
Reaction Steps
According to the procedure of example 2, by hydrogenation of 1.62 g (10.3 mmol) of 2-tert-butyl-2,5-dimethyl-2,5-dihydrofuran in the presence of 600 mg (0.56 mmol) of 10% palladium on activated charcoal. Kugelrohr distillation furnished at 45-50° C./20 mbar 1.37 g (82%) of the title compound as a colorless odoriferous liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07632790B2 |
| Source dataset | uspto-grants-2009_12 |
| ORD ID | ord-723c3052942b404a9dc3a5ca640a32eb |
| Source note | uspto-grants-2009_12 |