3-Bromopropionic acid → 3-bromo-N-methoxy-N-methylpropanamide

HRID 1867354Notes

Reaction equation

HRID 1867354 reaction equation
Br[CH2:2][C:3]([N:5]([O:7][CH3:8])[CH3:6])=[O:4].[Br:9][CH2:10]CC(O)=O>>[Br:9][CH2:10][CH2:2][C:3]([N:5]([O:7][CH3:8])[CH3:6])=[O:4]

Participants

3

Reactant 2

HCID 115533-Bromopropionic acidHCID 108669612-Bromo-N-methoxy-N-methylacetamide

Product 1

HCID 112063733-bromo-N-methoxy-N-methylpropanamide

Procedure

In analogy to the procedure described in intermediate 1D, 3-bromopropionic acid gave the title compound as a light yellow liquid. MS: 195.9 (MH+, 1Br).

Sources & evidence

ORD record
ord-3745cdc1664c4dec9a4eb5ca33c39cab
Source dataset
uspto-grants-2009_12
Patent number
US07632829B2

Reaction notes

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