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HRID1867449

反应详情

EQUATION

反应方程式

HRID 1867449 的结构方程式

REACTANTS

反应物

2
结构：CC1(C)OC[C@H](CCOS(C)(=O)=O)O1
HCID13194537

未命名化合物

结构：O=C1CCN(C(=O)/C=C/c2ccc(Cl)c(Cl)c2)CCN1
HCID62044921

未命名化合物

2 次

PRODUCTS

生成物

1
结构：O=C(/C=C/c1ccc(Cl)c(Cl)c1)N1CCC(=O)N(CC[C@H](O)CO)CC1
HCID68434131

未命名化合物

PROCEDURE

实验过程

In analogy to the procedure described for example 167A and 167B, 1-[(E)-3-(3,4-dichloro-phenyl)-acryloyl]-[1,4]diazepan-5-one (intermediate 1A]) and methanesulfonic acid 2-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-ethyl ester (prepared from 2-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-ethanol and methanesulfonyl chloride) gave the title compound as an white foam. MS: 401.3 (MH+, 2Cl).