3-Bromo-N,N-dimethylaniline → (3-Benzo[1,2,5]oxadiazol-5-yl-phenyl)-dimethyl-amine

HRID 1867506Notes

Reaction equation

HRID 1867506 reaction equation
[N:1]1[O:5][N:4]=[C:3]2[CH:6]=[C:7](B(O)O)[CH:8]=[CH:9][C:2]=12.Br[C:14]1[CH:15]=[C:16]([N:20]([CH3:22])[CH3:21])[CH:17]=[CH:18][CH:19]=1>>[N:1]1[O:5][N:4]=[C:3]2[CH:6]=[C:7]([C:14]3[CH:15]=[C:16]([N:20]([CH3:22])[CH3:21])[CH:17]=[CH:18][CH:19]=3)[CH:8]=[CH:9][C:2]=12

Participants

3

Reactant 2

HCID 1401023-Bromo-N,N-dimethylanilineHCID 4672597Benzo[C][1,2,5]Oxadiazole-5-Boronic Acid

Product 1

HCID 68878569(3-Benzo[1,2,5]oxadiazol-5-yl-phenyl)-dimethyl-amine

Procedure

Starting from 5-benzo[1,2,5]oxadiazoleboronic acid and (3-bromo-phenyl)-dimethyl-amine. Orange-yellow powder. MS(ES+): 240 (M+1).

Sources & evidence

ORD record
ord-817404acb450404a941d24f571e12da9
Source dataset
uspto-grants-2009_12
Patent number
US07632851B2

Reaction notes

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