5-Bromo-2,1,3-benzoxadiazole → HCID 68878052, compound

HRID 1867517Notes

Reaction equation

HRID 1867517 reaction equation
Br[C:2]1[CH:3]=[CH:4][C:5]2[C:6]([CH:10]=1)=[N:7][O:8][N:9]=2.C(O[C:16](=O)[N:17]([C:19]1[CH:24]=[CH:23][C:22](Br)=[C:21]([O:26][CH3:27])[CH:20]=1)C)(C)(C)C>>[N:9]1[O:8][N:7]=[C:6]2[CH:10]=[C:2]([C:22]3[CH:23]=[CH:24][C:19]([NH:17][CH3:16])=[CH:20][C:21]=3[O:26][CH3:27])[CH:3]=[CH:4][C:5]=12

Participants

3

Reactant 2

HCID 27762985-Bromo-2,1,3-benzoxadiazoleHCID 68878067HCID 68878067, compound

Product 1

HCID 68878052HCID 68878052, compound

Procedure

The starting compound is obtained according to the procedure described in Example 7 from 5-bromo-benzo[1,2,5]oxadiazole and (4-bromo-3-methoxy-phenyl)-methyl-carbamic acid tert-butyl ester, as a yellow powder. MS(ES+): 378 (M+23).

Workup

  1. customThe starting compound is obtained

Sources & evidence

ORD record
ord-a59e22c353bd46af8dbf77d046bc6834
Source dataset
uspto-grants-2009_12
Patent number
US07632851B2

Reaction notes

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