HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 69077690, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 67528883 | HCID 67528883 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 69077690 | HCID 69077690 | — |
Reaction Steps
A solution of 0.75 g (2.74 mmol) of 3-{2-[4-(trifluoromethyl)phenyl]ethyl}-1,3-oxazolidine-2,4-dione obtained in step 2.1., in 10 ml of methanol is admixed with 8 ml (16.47 mmol) of a solution (2M) of methylamine in tetrahydrofuran. Stirring is continued at ambient temperature for 12 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07632850B2 |
| Source dataset | uspto-grants-2009_12 |
| ORD ID | ord-8c15987a174f4330bf03349a6190d56c |
| Source note | uspto-grants-2009_12 |