Iodine → HCID 57762887, compound

HRID 1867661Notes

Reaction equation

HRID 1867661 reaction equation
[OH:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[C:9](=[O:21])[CH:10]=[CH:11][C:12]1[CH:17]=[C:16]([CH3:18])[C:15]([OH:19])=[C:14]([CH3:20])[CH:13]=1.II>CS(C)=O>[CH3:20][C:14]1[CH:13]=[C:12]([C:11]2[O:1][C:2]3[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=3[C:9](=[O:21])[CH:10]=2)[CH:17]=[C:16]([CH3:18])[C:15]=1[OH:19]

Participants

4

Reactant 2

HCID 807IodineHCID 66704477HCID 66704477, compound

Product 1

HCID 57762887HCID 57762887, compound

Reagents, catalysts & solvents 1

HCID 679Dimethyl SulfoxideSolvent

Procedure

1-[2-hydroxy-4-chlorophenyl]-3-[3,5-dimethyl-4-hydroxyphenyl]prop-2-en-1-one was dissolved in dimethylsulfoxide, an iodine crystal was added, and the mixture was kept under reflux for 10 min.

Workup

  1. temperatureunder reflux for 10 min.

Sources & evidence

ORD record
ord-fd637cc3a5d54241bcc6fb7e1831499c
Source dataset
uspto-grants-2009_12
Patent number
US07632870B2

Reaction notes

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