HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2S)-2-(((tert-butoxy)carbonyl)amino)-3-methoxypropanoic acid → HCID 86616946, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2S)-2-(((tert-butoxy)carbonyl)amino)-3-methoxypropanoic acid | HCID 7016354 | — |
| Reactant | HCID 11691173 | HCID 11691173 | — |
| Reactant | N-[(1,1-Dimethylethoxy)carbonyl]-O-methyl-L-homoserine | HCID 15058461 | — |
| Product | HCID 86616946 | HCID 86616946 | — |
Reaction Steps
The N2,O-dimethyl-L-homoserinamide used as starting material was prepared by methylating N-(tert-butoxycarbonyl)-O-methyl-L-homoserine using an analogous method to that described in Example 7 for the methylation of N-(tert-butoxycarbonyl)-O-methyl-L-serine, to give N-(tert-butoxycarbonyl)-N,O-dimethyl-L-homoserine; 1H NMR spectrum: (DMSO d6, 100° C.) 1.40 (s, 9H), 1.91 (m, 1H), 2.09 (m, 1H), 2.75 (s, 3H), 3.24 (s, 3H), 3.34 (m, 2H), 4.44 (m, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07632840B2 |
| Source dataset | uspto-grants-2009_12 |
| ORD ID | ord-93074dd4f2074680aac2ced2b85ccef8 |
| Source note | uspto-grants-2009_12 |