HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 11691173, compound → HCID 55283965, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 11691173 | HCID 11691173 | — |
| Reactant | HCID 86616946 | HCID 86616946 | — |
| Product | HCID 55283965 | HCID 55283965 | — |
Reaction Steps
N-(tert-butoxycarbonyl)-N,O-dimethyl-L-homoserine was converted to the corresponding amide, followed by removal of the nitrogen protecting group using an analogous as process to that described in Example 7 for the preparation of N2,O-dimethyl-L-serinamide, to give N2,O-dimethyl-L-homoserinamide; 1H NMR spectrum: (DMSO d6) 1.58 (m, 1H), 1.69 (m, 1H), 1.80 (brs, 1H), 2.17 (s, 3H), 2.84 (dd, 1H), 3.20 (s, 3H), 3.34 (m, 2H), 6.93 (brs, 1H), 7.27 (brs, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07632840B2 |
| Source dataset | uspto-grants-2009_12 |
| ORD ID | ord-ac49ee3a3c6c457abfcecfbed5394f01 |
| Source note | uspto-grants-2009_12 |