HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl bromide → HCID 23539493, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 2,7-Dibromofluorene | HCID 140073 | — |
| Reactant | HCID 57980924 | HCID 57980924 | — |
| Catalyst | Tetrabutylammonium Bromide | HCID 74236 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 23539493 | HCID 23539493 | — |
Reaction Steps
2,7-dibromofluorene (5 g, 15.4 mmol) was combined with allyl bromide (5.6 g, 46.2 mmol) and reacted with toluene, NaOH and Bu4NBr as above for 2,7-dibromo-9,9-dihex-5-enyl-fluorene. 7.1 g of a yellow solid was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07633220B2 |
| Source dataset | uspto-grants-2009_12 |
| ORD ID | ord-d1b0b079d0564442a19f61bf2995de37 |
| Source note | uspto-grants-2009_12 |