HCID 67100249, compound → HCID 57983570, compound

Participants

Reaction Steps

1,1-Dimethylethyl N-((6-methyl-4-hydroxy-1,1-dimethyl-2-oxo-naphthalen-3-yl)carbonyl)glycinate (255 mg, 709 μmol) was dissolved in TFA (3 mL) at ambient temperature for 30 minutes. The reaction mixture was then concentrated, precipitated with hexanes, filtered, and dried in a vacuum oven to give the title compound (192 mg) as a white solid. MS (m/z)=304 (M+H)+. Calculated for C16H17NO5 303.11.

Provenance & Evidence