Trifluoroacetic acid → HCID 57983360, compound

Participants

Reaction Steps

A solution of tert-butyl 2-(5-hydroxy-8,8-dimethyl-7-oxo-7,8-dihydroquinoline-6-carboxamido)acetate (15 mg) and TFA (1 mL) was stirred at room temperature. After 20 minutes, LCMS showed that the reaction was complete. The reaction was concentrated in vacuo to give a yellow oil. The sample was lyophilized to give a white solid (10 mg, 60%). MS (m/z)=291 (M+H)+. Calculated for C14H14N2O5 290.3.

Provenance & Evidence