HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylamine → HCID 23078911, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | Benzyl acrylate | HCID 75617 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23078911 | HCID 23078911 | — |
Reaction Steps
To a solution of benzyl acrylate (2 g) in ethanol (15 mL) was added benzylamine (1.75 mL), and the mixture was stirred at room temperature overnight. The reaction mixture was concentrated under reduced pressure, and the residue was purified by column chromatography on silica gel (eluent: n-hexane/ethyl acetate=2/1-1/1) to give the title compound (2.91 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07635684B2 |
| Source dataset | uspto-grants-2009_12 |
| ORD ID | ord-8974bc814beb4eb6bda7df3aefaeb6f6 |
| Source note | uspto-grants-2009_12 |