HuagongsheHuagongshe Chemistry Print Report · For research reference only
(1R)-3-chloro-1-phenylpropan-1-ol → HCID 57985886, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (1R)-3-chloro-1-phenylpropan-1-ol | HCID 642409 | — |
| Reactant | 7-Methoxy-1H-pyrrolo[3,2-b]pyridine | HCID 45079605 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 57985886 | HCID 57985886 | 33% |
Reaction Steps
1-(3-Chloro-1-(S)-phenyl-propyl)-7-methoxy-1H-pyrrolo[3,2-b]pyridine 79 was prepared from 7-methoxy-1H-pyrrolo[3,2-b]pyridine and 3-chloro-1-(R)-phenyl-propan-1-ol following the procedure of steps 1 and 2 of Example 11 (33% yield, 170 mg, [αD=−149° (CHCl3, c=1)])
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07638517B2 |
| Source dataset | uspto-grants-2009_12 |
| ORD ID | ord-fe912dc5797d43ed8d92929d9bfbac92 |
| Source note | uspto-grants-2009_12 |