HCID 178444001, compound → 1-(4-(3-bromophenyl)-1H-imidazol-2-yl)-5-methyl-1-hexanamine

Participants

Reaction Steps

tert-Butyl 1-(4-(3-bromophenyl)-1H-imidazol-2-yl)-5-methylhexylcarbamate (obtained at stage 13777.2; 3.5 g; 0.008 mol) was agitated in 120 ml of an ethyl acetate solution saturated in hydrochloric acid for about 2.5 at a temperature of about 55° C. The solid obtained was filtered and washed with ether. A white powder was obtained with a yield of 97%. Melting point: 200-202° C. MH+=336.2.

Provenance & Evidence