HRID1869566

反应详情

EQUATION

反应方程式

HRID 1869566 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

In analogy to the procedure carried out in example 1, 12 mol of 2-ethylhexanol were reacted with 8 mol of benzoic acid and tetrabutyl titanate. Distillation (3 mbar, overhead temperature 134° C.) gives 2-ethylhexyl benzoate in a purity, determined by gas chromatography, of 99.7%.

WORKUP

后处理

  1. distillationDistillation (3 mbar, overhead temperature 134° C.)