Benzene, (3-iodopropyl)- → 5-Phenyl-1-pentyne

HRID 1869686Notes

Reaction equation

HRID 1869686 reaction equation
[C:1]1([CH2:7][CH2:8][CH2:9]I)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[C-:11]#[C-:12].[Na+].[Na+]>>[C:1]1([CH2:7][CH2:8][CH2:9][C:11]#[CH:12])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

3

Reactant 2

HCID 138121Benzene, (3-iodopropyl)-HCID 178463197HCID 178463197, compound

Product 1

HCID 745735-Phenyl-1-pentyne

Procedure

The title compound was synthesized using 3-phenyl-1-iodopropane and sodium acetylide by conducting the reactions similar to those mentioned in Reference example 29.

Sources & evidence

ORD record
ord-3230ac5bb11943118d80d019d1baf41d
Source dataset
uspto-grants-2009_12
Patent number
US07638551B2

Reaction notes

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