HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1870239Generated: October 30, 2026
3-Hydroxybenzyl alcohol → HCID 54441959, compound
https://huagongshe.com/reaction/1870239
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 3-Hydroxybenzyl alcohol | HCID 102 | — |
| Reactant | HCID 18695876 | HCID 18695876 | — |
| Product | HCID 54441959 | HCID 54441959 | 30% |
Reaction Steps
A mixture of 2-chloromethyl-1-isocyanato-3-methylbenzene (2 g) and 3-hydroxybenzyl alcohol (1.6 g) is warmed to 75° C. in an oil bath for 1 h and then purified by chromatography on silica gel (eluent: dichloromethane/methanol 19:1). 1 g (30%) of the title compound is obtained as a crude product in the form of an amorphous solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06096758 |
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| Source dataset | uspto-grants-2000_08 |
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| ORD ID | ord-9a15a45af7db44df930239e39a143387 |
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| Source note | uspto-grants-2000_08 |
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