HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(3,5-dichlorophenyl)-D,L-alanine → N-[N-(3,5-dichlorophenyl)-D,L-alanyl]-(S)-2-aminohexanamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(3,5-dichlorophenyl)-D,L-alanine | HCID 15484844 | — |
| Reactant | BOC-Norleucine Amide | HCID 15609364 | — |
| Product | N-[N-(3,5-dichlorophenyl)-D,L-alanyl]-(S)-2-aminohexanamide | HCID 131721931 | — |
Reaction Steps
Following General Procedure D and using N-(3,5-dichlorophenyl)-D,L-alanine (from Example B above) and L-norleucine amide (from Example F above), the title compound was prepared. The reaction was monitored by tlc (Rf=0.15 in 3% methanol/dichloromethane) and purification of this compound was by thin layer chromatography with 3% methanol/dichloromethane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06096782 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-4d9f1f7bb06c46f48fb85208f792c91c |
| Source note | uspto-grants-2000_08 |