9-Decen-1-ol → (E)-3(4-Diethylamino-2-hydroxy-phenyl)-but-2-enoic acid dec-9-enyl ester

HRID 1870581Notes

Reaction equation

HRID 1870581 reaction equation
[CH2:1]([O:11][C:12](=[O:28])[CH:13]=[C:14]([C:16]1[CH:21]=[CH:20][C:19]([N:22]([CH2:25][CH3:26])[CH2:23][CH3:24])=[CH:18][C:17]=1[OH:27])[CH3:15])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH:9]=[CH2:10].C(OC(=O)C=C(C1C=CC(N(CC)CC)=CC=1O)C)C.C(O)CCCCCCCC=C>>[CH2:1]([O:11][C:12](=[O:28])/[CH:13]=[C:14](/[C:16]1[CH:21]=[CH:20][C:19]([N:22]([CH2:23][CH3:24])[CH2:25][CH3:26])=[CH:18][C:17]=1[OH:27])\[CH3:15])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH:9]=[CH2:10]

Participants

4

Reactant 3

HCID 256129-Decen-1-olHCID 540390873-(4-Diethylamino-2-hydroxy-phenyl)-but-2-enoic acid ethyl esterHCID 545498073-(4-Diethylamino-2-hydroxy-phenyl)-but-2-enoic acid dec-9-enyl ester

Product 1

HCID 68522096(E)-3(4-Diethylamino-2-hydroxy-phenyl)-but-2-enoic acid dec-9-enyl ester

Procedure

According to the same procedure, 3-(4-diethylamino-2-hydroxy-phenyl)-but-2-enoic acid dec-9-enyl ester was prepared from 3-(4-diethylamino-2-hydroxy-phenyl)-but-2-enoic acid ethyl ester, dec-9-en-1-ol and tetraisopropyl-o-titanate.

Sources & evidence

ORD record
ord-ae8f6cebb5854fe5a5799ba30c7d2e10
Source dataset
uspto-grants-2000_08
Patent number
US06096918

Reaction notes

Loading…