HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 18692792, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | HCID 18692816 | HCID 18692816 | — |
| Catalyst | Iron | HCID 23925 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18692792 | HCID 18692792 | — |
Reaction Steps
Iron powder (6.72 g), N,N-bis(3-hydroxypropyl)-4-nitrosoaniline (10 g) and hydrochloric acid(20cm3) in methanol (120cm3) were refluxed for 2hrs. The resulting mixture was made alkaline with sodium carbonate, filtered and the solvent removed to leave N,N-bis(3-hydroxypropyl)-4-aminoaniline as a brown solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06099625 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-32810475a56c4dff8dfce95c263526c8 |
| Source note | uspto-grants-2000_08 |