HuagongsheHuagongshe Chemistry Print Report · For research reference only
[2-(Pyridin-2-yl)-1,3-thiazol-4-yl]methanol → 2-(Pyridin-2-yl)-1,3-thiazole-4-carbaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | [2-(Pyridin-2-yl)-1,3-thiazol-4-yl]methanol | HCID 10750266 | — |
| Catalyst | Manganese oxide | HCID 160959 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 2-(Pyridin-2-yl)-1,3-thiazole-4-carbaldehyde | HCID 2125337 | 87.1% |
Reaction Steps
5.8 g of the product of Stage D in 60 ml of toluene were refluxed for 2 hours in the presence of 13 g of manganese oxide and filtration was carried out. The solvent was evaporated under reduced pressure to obtain 5 g of the expected product melting at 131° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06100404 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-b42905e4ec564df6a7543fa5dc85f48d |
| Source note | uspto-grants-2000_08 |