HCID 54124111, compound → HCID 18694808, compound

HRID 1871035Notes

Reaction equation

HRID 1871035 reaction equation
[N:1]1[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=1[C:7]1[S:8][CH:9]=[C:10]([CH:12]=[CH:13][CH2:14][CH2:15][N:16]2C(=O)C3C(=CC=CC=3)C2=O)[N:11]=1>[Pd]>[N:1]1[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=1[C:7]1[S:8][CH:9]=[C:10]([CH2:12][CH2:13][CH2:14][CH2:15][NH2:16])[N:11]=1

Participants

3

Reactant 1

HCID 54124111HCID 54124111, compound

Product 1

HCID 18694808HCID 18694808, compoundYield 135.8%

Reagents, catalysts & solvents 1

HCID 23938PalladiumCatalyst

Procedure

Using the procedure of Stage B of Preparation 32, 7.22 g of the product of Stage F and 1.5 g of palladium on activated charcoal were hydrogenated for 2 hours under 1800 mbars to obtain 6.33 g of the expected product melting at 119-121° C.

Sources & evidence

ORD record
ord-49da3a59ef1c4e169757940e06b4136f
Source dataset
uspto-grants-2000_08
Patent number
US06100404

Reaction notes

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