HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexanone Oxime → HCID 524012, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexanone Oxime | HCID 7517 | — |
| Reactant | Isopropenyl acetate | HCID 7916 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 524012 | HCID 524012 | 100% |
Reaction Steps
A mixture of 2.3 g (20 mmole) of cyclohexanone oxime, 2.0 g (20 mmole) of isopropenyl acetate, 0.9 g (2 mmole) of di(η5 -pentamethylcyclopentadienyl)samarium [Cp*2Sm(THF)2 ], and 20 ml of toluene was stirred at room temperature for one hour, and the precipitated crystals were filtered. 3.1 g of acetyloxyiminocyclohexane (O-acetylcyclohexanone oxime) (yield: 100%) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06100419 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-eb1e51eefc8f4c09867a941331695254 |
| Source note | uspto-grants-2000_08 |