HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18690802, compound → HCID 54422358, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18690802 | HCID 18690802 | — |
| Reactant | HCID 178418287 | HCID 178418287 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 54422358 | HCID 54422358 | 62% |
Reaction Steps
Prepared in an analogous manner to that described in Example 4, via oxidation of 2-(5-tert-butyl-1-indanyl)-1-ethanol (3.85 g, 17.6 mmole) in CH2Cl2 (40 ml), by means of PCC (5.73 g, 25 mmole) in CH2Cl2 (60 ml). After the treatment described and bulb-to-bulb distillation (150°/40 Pa), there was obtained the desired carbaldehyde (2.34 g, yield 62%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06103688 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-f8318ecc264341918ea27090a918e7af |
| Source note | uspto-grants-2000_08 |