HuagongsheHuagongshe Chemistry Print Report · For research reference only
cis-4-(3,4-Dimethoxyphenyl)-4a,5,8,8a-tetrahydro-2H-phthalazin-1-one → (cis)-2-(4-Propyl-butyl)-4-(3,4-dimethoxyphenyl)-4a,5,8,8a-tetrahydro-2H-phthalazin-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | cis-4-(3,4-Dimethoxyphenyl)-4a,5,8,8a-tetrahydro-2H-phthalazin-1-one | HCID 10935039 | — |
| Reactant | (Heptan-4-yl)hydrazine | HCID 19367998 | — |
| Reactant | (cis)-4-(3,4-Dimethoxyphenyl)-2-methyl-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-one | HCID 70003942 | — |
| Product | (cis)-2-(4-Propyl-butyl)-4-(3,4-dimethoxyphenyl)-4a,5,8,8a-tetrahydro-2H-phthalazin-1-one | HCID 70003479 | — |
Reaction Steps
Prepared from compound 3 and 4-heptylhydrazine as described for compound 8. Purified by chromatography and crystallized from petroleum ether (60-80° C.) M.p. 71-73° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06103718 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-38ca16b945714725a73995c97a13620b |
| Source note | uspto-grants-2000_08 |