HRID1871372

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID16992

Cycloheptane, bromo-

C7H13Br

结构：COc1ccc(C2=NNC(=O)[C@H]3CC=CC[C@@H]23)cc1OC

HCID10935039

未命名化合物

结构：COc1ccc(C2=NN(C)C(=O)[C@H]3CCCC[C@@H]23)cc1OC

HCID70003942

未命名化合物

PRODUCTS

生成物

结构：COc1ccc(C2=NN(C3CCCC3)C(=O)[C@H]3CC=CC[C@@H]23)cc1OC

HCID70002499

未命名化合物

PROCEDURE

实验过程

Prepared from compound 3 and cycloheptylbromide as described for compound 8. Purified by chromatography (dichloromethane) and crystallized from diethyl ether. M.p. 131-133° C.

WORKUP

后处理

customPurified by chromatography (dichloromethane)
customcrystallized from diethyl ether