HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromocycloheptane → (cis)-4-(3-Cyclopentyloxy-4-methoxyphenyl)-2-cycloheptyl-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromocycloheptane | HCID 16992 | — |
| Reactant | (cis)-4-(3-Cyclopentyloxy-4-methoxyphenyl)-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-one | HCID 11727597 | — |
| Reactant | (cis)-4-(3,4-Dimethoxyphenyl)-2-methyl-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-one | HCID 70003942 | — |
| Product | (cis)-4-(3-Cyclopentyloxy-4-methoxyphenyl)-2-cycloheptyl-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-one | HCID 70106724 | — |
Reaction Steps
Prepared from compound 4 and cycloheptylbromide as described for compound 8. Crystallized from petroleum ether (60-80° C.) M.p.111-112° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06103718 |
| Source dataset | uspto-grants-2000_08 |
| ORD ID | ord-3568d7aa370d448b990b840b9e46325a |
| Source note | uspto-grants-2000_08 |