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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1871378Generated: November 3, 2026

Allyl chloride → HCID 70001391, compound

https://huagongshe.com/reaction/1871378

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAllyl chlorideHCID 7850—
Reactant(cis)-4-(3,4-Dimethoxyphenyl)-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-oneHCID 10913208—
Reactant(cis)-4-(3,4-Dimethoxyphenyl)-2-methyl-4a,5,6,7,8,8a-hexahydro-2H-phthalazin-1-oneHCID 70003942—
ProductHCID 70001391HCID 70001391—

Reaction Steps

Prepared from compound 1 and allylchloride as described for compound 8. Purified by chromatography (dichloromethane). Crystallized from petroleum ether (60-95° C.). M.p. 99-101° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06103718
Source datasetuspto-grants-2000_08
ORD IDord-aaac3dae66ee48c78530e44c6d6339c2
Source noteuspto-grants-2000_08